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Physics Science College, Qingdao University, Qingdao 266071, China; 2. Key Laboratory of Photonics Materials and Technology in Universities of Shandong, Qingdao Uni- versity, Qingdao 266071, China; 3. Institute of Complexity Science, Qingdao University, Qingdao 266071, China; 4. Beijing Synchrotron Radiation Laboratory, Institute of High Energy, Beijing 100039, China）<br /> 机构地区：[1]青岛大学物理科学学院,山东青岛266071 [2]山东省高校光子学材料与技术重点实验室,青岛大学,山东青岛266071 [3]青岛大学复杂性科学研究所,山东青岛266071 [4]中科院高能物理研究所北京同步辐射实验室,北京100039<br /> 出 处：《中国稀土学报》 CSCD 2015年第33卷第1期 53-59页,共7页<br /> Journal of the Chinese Rare Earth Society<br /> 基 金：国家自然科学基金项目（11204148,11274188,11374170）; 山东省优秀中青年科学家奖励基金项目（BS2013CL024）资助<br /> 摘 要：采用提拉法生长出了Yb：YxLu1-xVO4混合晶体,XRD测试发现该晶体具有四方Zr Si O4结构,经计算晶胞常数为a=b=0.7126（2）nm,c=0.6259（7）nm。利用化学腐蚀法和同步辐射X射线形貌术,分析了晶体中的缺陷,发现位错和小角度晶界是晶体中的两种主要缺陷。利用Read-Shockley公式计算分析了晶体中的转向小角度晶界,发现Yb：YxLu1-xVO4晶体中存在伯格斯矢量为[100]的位错。分析了晶体中位错和小角度晶界的形成原因,认为晶体生长和退火过程中的温度波动容易在Yb：YxLu1-xVO4晶体内部引起局部晶格畸变,诱发位错和小角度晶界的产生,因此混合晶体生长过程需要更精确控制。<br /> Mixed Yb ：YxLU1-xVO4 crystal was grown by Czochralski method. XRD showed that this crystal possessed tetragonal ZrSiO4 structure. The lattice parameters are a = b =0. 7126（2） nm, c =0.6259（7） nm. Crystal defects were revealed by chemical etching and Synchrotron Radiation X-ray Topography. It was found that dislocations and low angle grain boundaries were dominated defects. Read-Shockley formula was used to analyze the low angle grain boundaries that changed in directions. It was found that there were dislocations with Burgers vector [ 100 ] in mixed Yb：YxLu1-xVO4 crystals. The formation reasons of dislocations and low angle grain boundaries were discussed. It is believed that the temperature fluctuation during crystal growth and annealing heat treatment, gave rise to the lattice deformation, which might induce dislocations and low angle grain boundaries. Thus, the processes of mixed crystal growth need more accurate control.<br /> 关键词：Yb：YxLu1-xVO4混合晶体 晶体缺陷 激光晶体 同步辐射X射线形貌术 稀土<br /> Yb：YxLu1-xVO4 mixed crystal ; crystal defects ; laser crystal ; synchrotron radiation X-ray topography ; rare earths ;</div> <div style="height200px;"></div> </div> </div> </div> </div></div> </div> <!--autocomment filter by maxnum--> <div class="ft_wp"> <div id="ft" class=" cl"> <div id="flk" > <p> <a href="http://wpa.qq.com/msgrd?V=3&Uin=20600600&Site=光电工程师社区&Menu=yes&from=discuz" target="_blank" title="QQ"><img src="static/image/common/site_qq.jpg" alt="QQ" /></a><span class="pipe">|</span><a href="http://m.oecr.com" >手机版</a><span class="pipe">|</span><a href="http://so.oecr.com" title="站内搜索" target="_blank" >搜索</a><span class="pipe">|</span><a href="http://www.focaloptics.com" title="主办单位：武汉焦点光学技术有限公司" target="_blank" >焦点光学</a><span class="pipe">|</span><a href="http://www.oecr.com" target="_blank">光电工程师社区</a> ( <a href="http://beian.miit.gov.cn/" target="_blank">鄂ICP备17021725号-1</a> <a href="http://www.beian.gov.cn/portal/registerSystemInfo?recordcode=42011102000821" target="_blank">鄂网安备42011102000821号</a> ) <span id="tcss"></span><script type="text/javascript" src="http://tcss.qq.com/ping.js?v=1eOg" charset="utf-8"></script><script type="text/javascript" reload="1">pgvMain({"discuzParams":{"r2":"1028778","ui":0,"rt":"plugin","pn":1,"qq":"000"},"extraParams":""});</script></p> <p class="xs0"> <span id="debuginfo"> Copyright 2015 光电工程师社区 版权所有 All Rights Reserved. </span> </p> </div> <div id="ftl" > <p>申明：本站为非盈利性公益个人网站，已关闭注册功能，本站所有内容均为网络收集整理，不代表本站立场。如您对某些内容有质疑或不快，请及时联系我们处理！ </p> </div> <div id="frt" > <div class="wp"> <p class="dd01"> © 2001-2022 <a href="http://www.oecr.com" target="_blank">光电工程师社区</a> 网站备案号：<a href="https://beian.miit.gov.cn/">鄂ICP备17021725号</a> 网站公安备案号：<a href="http://www.beian.gov.cn/portal/registerSystemInfo?recordcode=42011102000821">鄂42011102000821号</a> Powered by <a href="http://www.discuz.net" target="_blank">Discuz!</a> <em>X3.2</em> </p><p class="dd02">GMT+8, 2025-12-17 05:39 </p> </div> </div></div> </div> </div> <!--bottombg结束--> <script src="home.php?mod=misc&ac=sendmail&rand=1765921154" type="text/javascript"></script> <!--<div id="scrolltop"> <span hidefocus="true"><a title="返回顶部" onclick="window.scrollTo('0','0')" class="scrolltopa" ><b>返回顶部</b></a></span> </div> --> <div id="scrolltop"> <span hidefocus="true"><a title="返回顶部" onclick="window.scrollTo('0','0')" class="scrolltopa" ><b>返回顶部</b></a></span> </div> <script type="text/javascript">_attachEvent(window, 'scroll', function () { showTopLink(); });checkBlind();</script> <div id="discuz_tips" style="display:none;"></div> <script type="text/javascript"> var tipsinfo = '1028778|X3.2|0.6||0||0|7|1765921154|3f4bf5c483dc1de811459c4c43724579|2'; </script> <script src="http://discuz.gtimg.cn/cloud/scripts/discuz_tips.js?v=1" type="text/javascript" charset="UTF-8"></script></body></html>